A wiped film evaporator (WFE), also known as a thin
film evaporator or agitated thin film
evaporator, is a specialized piece of equipment used in the separation of mixtures
based on
differences in volatility. It is particularly effective for processing
heat-sensitive, viscous, or
thermally unstable materials, making it a popular choice in industries such as
pharmaceuticals, chemicals, food processing, and petrochemicals.
Working Principle
- Prevention of Scaling and Fouling:
The high velocity of liquid circulation reduces the risk of scaling and fouling
on the heat exchanger surfaces, even with solutions prone to crystallization.
- Introduction of Feed: The feed
mixture,
typically a liquid containing volatile and nonvolatile components, is
introduced into the evaporator through an inlet at the top.
- Film Formation: The feed is evenly
distributed onto the inner surface of a heated
cylindrical wall by a rotating wiper blade mechanism. This wiper system
continuously
spreads the liquid into a thin film, typically in the range of 0.1 to 1.0 mm
thickness.
- Evaporation: As the thin film of
liquid
flows downward under the influence of gravity
and the wiper blades, the volatile components evaporate quickly due to the
high
surface area and close contact with the heated wall. The low residence time
and the thin film ensure that heat-sensitive materials are not exposed to high
temperatures for prolonged periods.
- Separation of Vapors: The
evaporated vapors
are then directed to a condenser,
where they are condensed into a liquid form and collected as distillate. The
nonvolatile components (residue) continue to flow downward along the wall
and are
collected at the bottom of the evaporator.
- Discharge: The residue, which is
typically
more viscous, is discharged from the
bottom outlet, while the distillate is collected separately.
Features of Wiped Film Evaporators
- Low Residence Time: The short
residence time of the product in the evaporator
minimizes thermal degradation, making WFE ideal for heat-sensitive materials.
- Handling of High Viscosity: WFEs
are capable of handling highly viscous liquids,
slurries, and materials that may be challenging to process in other types of
evaporators.
- Vacuum Operation: WFEs can operate
under vacuum conditions, which lowers the
boiling point of the volatile components, further protecting heat-sensitive
materials.
- Scalability: Wiped film
evaporators are available in various sizes, from lab-scale units
for R&D to large industrial-scale systems.
- Minimal Fouling: The wiping action
reduces the risk of fouling or scaling on the
heated surface, maintaining consistent heat transfer efficiency.
- High Purity Separation: WFEs can
achieve high levels of purity in the separated
components due to the precise control of operating conditions.
- Flexibility: They are suitable for
a wide range of applications, including distillation,
stripping, and solvent recovery
Applications of Wiped Film Evaporators
- Pharmaceuticals: Purification of
active pharmaceutical ingredients (APIs),
concentration of heat-sensitive compounds, and removal of solvents from drug
formulations.
- Chemicals: Separation and
purification of fine chemicals, resins, polymers, and
specialty chemicals.
- Food and Beverage: Concentration
of flavors, fragrances, essential oils, and natural
extracts.
- Petrochemicals: Recovery of
valuable hydrocarbons, removal of volatile impurities
from oils, and purification of lubricants.
- Biotechnology: Processing of
bio-based materials, including the concentration of
enzymes, proteins, and other biological products.
Advantages of Wiped Film Evaporators
- Gentle Processing: Ideal for heat-sensitive materials due to the short residence time
and the ability to operate at low temperatures.
- High Efficiency: Capable of achieving high separation efficiency with minimal loss of
product quality.
- Versatility: Suitable for a wide range of applications, from simple distillation to
complex purification processes.
- Scalable: Can be used in both small-scale laboratory settings and large-scale
industrial production.